激光冲击强化对镍基单晶高温合金微观组织和抗高温氧化性能的影响

doi:10.11902/1005.4537.2023.392

中国腐蚀与防护学报

2024, Vol. 44

Issue (5): 1295-1304 CSTR: 32134.14.1005.4537.2023.392 DOI: 10.11902/1005.4537.2023.392

研究报告

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激光冲击强化对镍基单晶高温合金微观组织和抗高温氧化性能的影响

李佳恒¹^,², 钱伟¹^,², 朱晶晶¹^,², 蔡杰¹^,², 花银群¹^,²(

)

1 江苏大学先进制造与现代装备技术工程研究院镇江 212013
2 江苏大学机械工程学院镇江 212013

Influence of Laser Shock Peening on Microstructure and Oxidation Performance of Nickel-based Single Crystal Superalloy

LI Jiaheng¹^,², QIAN Wei¹^,², ZHU Jingjing¹^,², CAI Jie¹^,², HUA Yinqun¹^,²(

)

1 Institute of Advanced Manufacturing and Modern Equipment Technology, Jiangsu University, Zhenjiang 212013, China
2 School of Mechanical Engineering, Jiangsu University, Zhenjiang 212013, China

引用本文:

李佳恒, 钱伟, 朱晶晶, 蔡杰, 花银群. 激光冲击强化对镍基单晶高温合金微观组织和抗高温氧化性能的影响[J]. 中国腐蚀与防护学报, 2024, 44(5): 1295-1304.
Jiaheng LI, Wei QIAN, Jingjing ZHU, Jie CAI, Yinqun HUA. Influence of Laser Shock Peening on Microstructure and Oxidation Performance of Nickel-based Single Crystal Superalloy[J]. Journal of Chinese Society for Corrosion and protection, 2024, 44(5): 1295-1304.

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摘要:

研究了激光冲击强化(LSP)对镍基单晶高温合金微观结构和氧化性的影响，首先对试样进行LSP处理，随后将试样置于980℃下进行10和150 h的氧化实验，对比分析了原始和LSP试样的微观结构、显微硬度和氧化形貌演变，最后探讨了LSP对该合金氧化性能的影响。结果表明，1次冲击后，样品表面引入了网状分布的位错，表面显微硬度从原始的420 HV增加到495 HV；3次冲击后，表面位错分布更加均匀密集，出现了位错缠结，表面显微硬度增加到约590 HV。此外，LSP在表面产生的位错为氧化过程提供了扩散通道，促进了连续的保护性氧化膜的形成，从而减少了贫Al孔洞的形成并增加了氧化膜抗剥落能力。

关键词 ：激光冲击强化, 微观演变, 镍基单晶高温合金, 元素扩散, 氧化

Abstract：

The impact of laser shock peening (LSP) on the microstructure and oxidation behavior of the nickel-based single crystal superalloy was investigated. The samples underwent LSP treatment, followed by oxidation for 10 and 150 h at 980^oC. The microstructure, microhardness, and oxidation morphology of this alloy without and with LSP treatment were comparatively examined. Finally, the mechanism by which LSP affects the oxidation behavior of this alloy was elucidated. The result shows that after a single impact, the surface of the specimen manifested some grid-like dislocations distribution, alongside an increment in microhardness from an initial value of 420 HV to 495 HV. After three impacts, the dislocations on the surface appeared more uniformly distributed with evident entanglement, culminating in an elevation of surface microhardness to approximately 590 HV. Furthermore, the dislocations generated on the surface by LSP promoted the formation of diffusion pathways during the oxidation process, which facilitated the early formation of a continuous protective oxide scale. It decreased the formation of poor Al pits, which resulted from the development of a protective oxide scale in the subsequent stages of oxidation, thereby reducing the spalling of the oxide scale.

Key words： laser shock peening microstructural evolution nickel-based single crystal superalloy element diffusion oxidation

收稿日期: 2023-12-20 32134.14.1005.4537.2023.392

ZTFLH:

TN249

基金资助:国家自然科学基金(51641102)

通讯作者: 花银群，E-mail：huayq@ujs.edu.cn，研究方向为热障涂层及功能表面

Corresponding author: HUA Yinqun, E-mail: huayq@ujs.edu.cn

作者简介: 李佳恒，女，1999年生，硕士生

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https://www.jcscp.org/CN/10.11902/1005.4537.2023.392 或 https://www.jcscp.org/CN/Y2024/V44/I5/1295

图1 LSP工作原理和冲击路径示意图

图2 不同条件LSP处理后镍基单晶高温合金的微观结构与成分TEM分析

图3 不同条件LSP处理后镍基单晶高温合金截面的硬度变化

图4 未处理和LSP处理的镍基单晶高温合金的加载-卸载曲线以及表面纳米硬度与弹性模量

图5 未经以及经过LSP处理的镍基单晶高温合金表面XRD谱图

图6 镍基单晶高温合金在980℃下氧化10和150 h后的XRD结果

图7 UT、LSP-1和LSP-3镍基单晶高温合金试样在980℃下氧化10 h后的表面和截面形貌

表1 UT、LSP-1和LSP-3镍基单晶高温合金试样氧化10 h后表面成分 (atomic fraction / %)

图8 UT、LSP-1和LSP-3镍基单晶高温合金试样在980℃下氧化150 h后的表面和截面形貌

表2 UT、LSP-1和LSP-3镍基单晶高温合金试样氧化150 h后的表面成分 (atomic fraction / %)

图9 LSP后镍基单晶高温合金的位错变化

图10 未经以及经过LSP处理的镍基单晶高温合金氧化机理示意图

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