Long-term Corrosion of Lubricant Infused Surface with Micro-nano Structures on Anodized Aluminum Oxide

doi:10.11902/1005.4537.2023.154

Journal of Chinese Society for Corrosion and protection

2023, Vol. 43

Issue (4): 773-780 DOI: 10.11902/1005.4537.2023.154

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Long-term Corrosion of Lubricant Infused Surface with Micro-nano Structures on Anodized Aluminum Oxide

HU Qian, GAO Jiayi, GUO Ruisheng, SHI Junqin, WANG Xianzong(

)

Center of Advanced Lubrication and Seal Materials, Northwestern Polytechnical University, Xi'an 710072, China

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Abstract

Three double-layered lubricant infused surface (LIS) with different micro-nano structures (nanopores, enlarged nanopores, nanowires) on high purity Al-plates were prepared through anodizing for different times, and then filled with PAO oil. The effect of the structure of anodizing oxide films on the hydrophobicity, corrosion resistance, and stability of the prepared LISs were characterized by scanning electron microscopy (SEM), contact angle measurements, electrochemical impedance spectroscopy (EIS), and corrosion test in simulated seawater. The results showed that the |Z|_{0.01 Hz} of nanowires-LIS was still stable at 10⁸ Ω∙cm² after immersion in 1 mol/L NaCl for 240 d, showing more stable in long-term immersion corrosion test rather than the nanopores- and enlarged nanopores-LISs. Theoretical analysis showed that the nanowires-structure could store more PAO oil, and the blocking effect of its compact structure and high interaction energy with the oil greatly slow down the loss of PAO, so that the nanowires-LIS showed improved corrosion resistance and stability.

Key words: micro-nano structure anodizing anodized aluminum oxide (AAO) lubricant infused surface (LIS) corrosion resistance stability

Received: 09 May 2023 32134.14.1005.4537.2023.154

ZTFLH:

TG172

Fund: National Natural Science Foundation of China(51901188);Fundamental Research Funds for the Central Universities

Corresponding Authors: WANG Xianzong, E-mail: xianzong.wang@nwpu.edu.cn

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	HU Qian
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	SHI Junqin
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Cite this article:

HU Qian, GAO Jiayi, GUO Ruisheng, SHI Junqin, WANG Xianzong. Long-term Corrosion of Lubricant Infused Surface with Micro-nano Structures on Anodized Aluminum Oxide. Journal of Chinese Society for Corrosion and protection, 2023, 43(4): 773-780.

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https://www.jcscp.org/EN/10.11902/1005.4537.2023.154 OR https://www.jcscp.org/EN/Y2023/V43/I4/773

Fig.1 Schematic illustration of the preparation process of the coatings

Fig.2 SEM images of AAO templates with the microstructures of micron multi-face (a, e), NPs (b, f), enlarged NPs (c, g), and NWs (d, h)

Fig.3 Contact angles of micron multi-face, NPs, enlarged NPs and NWs without and with lubricant (a), and the sliding images of NWs+PAO at 25° (b1, b2)

Fig.4 Bode plots of fresh Al, micron multi-face and AAO without and with lubricant (a), and |Z|_{0.01 Hz} values of each sample (b)

Fig.5 Nyquist (a1-c1) and Bode (a2-c2) plots of NPs+PAO (a1, a2), Enlarged NPs+PAO (b1, b2), and NWs+PAO (c1, c2) after immersion for different time

Fig.6 |Z|_{0.01 Hz}curves of various samples during long-term immersion

Fig.7 Contact angles of various samples before and after immersion (a), and the sliding images of Enlarged NPs+PAO after immersion at 25° (b1, b2)

Fig.8 SEM surface images of NWs+PAO (a, e), NPs+PAO (b, f), enlarged NPs+PAO (c, g) and NWs+PAO (d, h) before (a-d) and after (e-h) immersion

Fig.9 Simulation results of filling of PAO oil in AAO templates with the microstructures of NPs (a1-a3), Enlarged NPs (b1-b3) and NWs (c1-c3)

Fig.10 Interaction energy curves of lubricant infused surfaces of NPs, enlarged NPs and NWs samples

Fig.11 Schematic diagrams of changes in corrosion resistance for NPs+PAO (a), Enlarged NPs+PAO (b) and NWs+PAO (c) samples during long-term immersion

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