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Journal of Chinese Society for Corrosion and protection  2024, Vol. 44 Issue (5): 1295-1304    DOI: 10.11902/1005.4537.2023.392
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Influence of Laser Shock Peening on Microstructure and Oxidation Performance of Nickel-based Single Crystal Superalloy
LI Jiaheng1,2, QIAN Wei1,2, ZHU Jingjing1,2, CAI Jie1,2, HUA Yinqun1,2()
1 Institute of Advanced Manufacturing and Modern Equipment Technology, Jiangsu University, Zhenjiang 212013, China
2 School of Mechanical Engineering, Jiangsu University, Zhenjiang 212013, China
Cite this article: 

LI Jiaheng, QIAN Wei, ZHU Jingjing, CAI Jie, HUA Yinqun. Influence of Laser Shock Peening on Microstructure and Oxidation Performance of Nickel-based Single Crystal Superalloy. Journal of Chinese Society for Corrosion and protection, 2024, 44(5): 1295-1304.

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Abstract  

The impact of laser shock peening (LSP) on the microstructure and oxidation behavior of the nickel-based single crystal superalloy was investigated. The samples underwent LSP treatment, followed by oxidation for 10 and 150 h at 980oC. The microstructure, microhardness, and oxidation morphology of this alloy without and with LSP treatment were comparatively examined. Finally, the mechanism by which LSP affects the oxidation behavior of this alloy was elucidated. The result shows that after a single impact, the surface of the specimen manifested some grid-like dislocations distribution, alongside an increment in microhardness from an initial value of 420 HV to 495 HV. After three impacts, the dislocations on the surface appeared more uniformly distributed with evident entanglement, culminating in an elevation of surface microhardness to approximately 590 HV. Furthermore, the dislocations generated on the surface by LSP promoted the formation of diffusion pathways during the oxidation process, which facilitated the early formation of a continuous protective oxide scale. It decreased the formation of poor Al pits, which resulted from the development of a protective oxide scale in the subsequent stages of oxidation, thereby reducing the spalling of the oxide scale.
Key words:  laser shock peening      microstructural evolution      nickel-based single crystal superalloy      element diffusion      oxidation     
Received:  20 December 2023      32134.14.1005.4537.2023.392
ZTFLH:  TN249  
Fund: National Natural Science Foundation of China(51641102)
Corresponding Authors:  HUA Yinqun, E-mail: huayq@ujs.edu.cn
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LI Jiaheng
QIAN Wei
ZHU Jingjing
CAI Jie
HUA Yinqun

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https://www.jcscp.org/EN/10.11902/1005.4537.2023.392     OR     https://www.jcscp.org/EN/Y2024/V44/I5/1295

Fig.1  Schematic diagrams of LSP working principle (a) and shocking route (b)
Fig.2  TEM micrographs (a-c) and mapping results (a1-c1) of nickel-based single crystal superalloy treated by LSP under different conditions: (a, a1) UT, (b, b1) LSP-1, (c, c1) LSP-3
Fig.3  Changes of microhardness with depth for nickel-based single crystal superalloy samples untreated and treated by LSP
Fig.4  Loading-unloading curves (a) and surface nano-hardnesses and elastic moduli (b) of nickel-based single crystal superalloy without and with LSP treatments
Fig.5  Surface XRD patterns of nickel-based single crystal superalloy without and with LSP treatments
Fig.6  Surface XRD patterns of nickel-based single crystal superalloy oxidized at 980oC for 10 h (a) and 150 h (b)
Fig.7  Surface (a-c) and cross-sectional (a1-c1) morphologies of UT (a, a1), LSP-1 (b, b1) and LSP-3 (c, c1) nickel-based single crystal superalloy samples after 10 h oxidation at 980oC
PositionNiAlCrCoO
Point 135.445.092.83.5153.16
Point 244.142.43.15.5444.82
Point 340.520.502.516.2750.20
Table 1  Surface chemical compositions of UT, LSP-1 and LSP-3 nickel-based single crystal superalloy samples after 10 h oxidation
Fig.8  Surface (a-c, a1-c1) and cross-sectional (a2-c2) morphologies of UT (a, a1, a2), LSP-1 (b, b1, b2) and LSP-3 (c, c1, c2) nickel-based single crystal superalloy samples after 150 h oxidation at 980℃
PositionNiAlCrCoTaOW
Point 140.280.718.636.40.0343.80.15
Point 216.2125.797.715.720.0744.460.04
Point 365.54.379.3412.520.974.72.6
Point 444.510.220.946.450.0647.740.08
Point 546.100.310.704.680.0148.170.03
Table 2  Surface chemical compositions of UT, LSP-1 and LSP-3 nickel-based single crystal superalloy samples after 150 h oxidation
Fig.9  Evolutions of dislocations in nickel-based single crystal superalloy after LSP treatments: (a)UT, (b) LSP-1, (c) LSP-3
Fig.10  Schematic diagrams of oxidation mechanism of nickel-based single crystal superalloy untreated (a) and treated (b) by LSP
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