Fabrication of Superamphiphobic Surface for Nickel-plate on Pipeline Steel by Salt Solution Etching and Its Anti-corrosion Properties

doi:10.11902/1005.4537.2020.008

Journal of Chinese Society for Corrosion and protection

2021, Vol. 41

Issue (1): 96-100 DOI: 10.11902/1005.4537.2020.008

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Fabrication of Superamphiphobic Surface for Nickel-plate on Pipeline Steel by Salt Solution Etching and Its Anti-corrosion Properties

HUANG Peng, GAO Rongjie(

), LIU Wenbin, YIN Xubao

School of Materials Science and Engineering, Ocean University of China, Qingdao 266100, China

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Abstract

A Ni-plate was firstly electrodeposited on X65 pipeline steel surface, which then was chemically etched by salt solution, and finally subjected to modification treatment with perfluorohexylethyltrichlorosilane, so that the surface of Ni-plate was endowed with super-hydrophobic and oil-phobic performance. The corrosion behavior of the modified Ni-plate was studied by potentiodynamic scanning. The result showed that after being etched for 6 h at 80 ℃ in the solution containing cobalt and nickel ions, and modified with perfluorooctyltrichlorosilane for 2 h, the modified Ni-plate surface presented contact angles of 160° and 152° for deionized water and glycol respectively. Compared with the original Ni-plate surface, the modified ones presented significantly lower corrosion rate, namely, better corrosion resistance.

Key words: salt solution etching Ni-plate superamphiphobic contact angle anti-corrosion property

Received: 17 February 2020

ZTFLH:

TG174.4

Fund: National Natural Science Foundation of China-Shandong Province Joint Fund(U1706221)

Corresponding Authors: GAO Rongjie E-mail: dmh206@ouc.edu.cn

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HUANG Peng, GAO Rongjie, LIU Wenbin, YIN Xubao. Fabrication of Superamphiphobic Surface for Nickel-plate on Pipeline Steel by Salt Solution Etching and Its Anti-corrosion Properties. Journal of Chinese Society for Corrosion and protection, 2021, 41(1): 96-100.

URL:

https://www.jcscp.org/EN/10.11902/1005.4537.2020.008 OR https://www.jcscp.org/EN/Y2021/V41/I1/96

Fig.1 SEM images of the Nickel-plated surface of X65 pipeline steel after salt solution etching for 6 h (a), magnified images of Fig.4a (b, c) and the surface without etching (d)

Fig.2 Contact angles of deionized water (a, c) and glycol (b, d) on the original surface (a, b) of nickel plating and superamphiphobic surface (c, d) of X65 pipeline steel

Fig.3 XRD patterns of Ni-plated surface of X65 pipeline steel after salt etching

Fig.4 Potentiodynamic polarization curves for the original surface, salt solution etching surface and superam-phiphobic surface in 3.5%NaCl solution

Table 1 Fitting electrochemical parameters of the potentiodynamic curves of the original surface, salt solution etching surface and superamphiphobic surface

Fig.5 Electrochemical impedance spectroscopy of the Ni-plated specimen and superam-phiphobic specimen in 3.5%NaCl solution

Table 2 Electrochemical model parameters obtained by fitting the Nyquist plots of the Nickel-plated specimen and superamphiphobic specimen

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