Effect of Microstructure on Hydrogen Induced Cracking and Hydrogen Trapping Behavior of X100 Pipeline Steel

doi:10.11902/1005.4537.2018.168

Journal of Chinese Society for Corrosion and protection

2019, Vol. 39

Issue (6): 536-542 DOI: 10.11902/1005.4537.2018.168

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Effect of Microstructure on Hydrogen Induced Cracking and Hydrogen Trapping Behavior of X100 Pipeline Steel

YUAN Wei,HUANG Feng(

),GAN Lijun,GE Fangyu,LIU Jing

State Key Laboratory of Refractories and Metallurgy, Wuhan University of Science and Technology, Wuhan 430081, China

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Abstract

The hydrogen induced cracking (HIC) sensitivity of X100 pipeline steels with different microstructures was evaluated according to the NACE TM 0284-2011 standard. While, the initiation and propagation of HIC, and the aggregation of hydrogen atoms in the steel were characterized via field emission scanning electron microscopy (FE-SEM) and hydrogen microprint technique. The relationship between hydrogen trapping efficiency and HIC sensitivity of X100 pipeline steels with different microstructure was analyzed by using kinetic parameters of hydrogen permeation. The results show that the HIC susceptibility of X100 pipeline steels with different microstructure could be ranked as follows: original specimen with ferrite-bainite microstructure＞furnace-cooling specimen with massive ferrite microstructure＞wind-cooling specimen with acicular ferrite microstructure. The microstructure has higher trapping efficiency, the more susceptible to HIC is. Hydrogen atoms tend to aggregate at the interface between inclusion and matrix, and the HIC could initiate at MnS inclusion, Ca-Al-Si-O composite inclusion and MnO inclusion in the steels.

Key words: X100 pipeline steel microstructure HIC susceptibility hydrogen trapping

Received: 13 November 2018

ZTFLH:

TG174

Fund: National Natural Science Foundation of China(51871172)

Corresponding Authors: Feng HUANG E-mail: Huangfeng@wust.edu.cn

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Cite this article:

YUAN Wei,HUANG Feng,GAN Lijun,GE Fangyu,LIU Jing. Effect of Microstructure on Hydrogen Induced Cracking and Hydrogen Trapping Behavior of X100 Pipeline Steel. Journal of Chinese Society for Corrosion and protection, 2019, 39(6): 536-542.

URL:

https://www.jcscp.org/EN/10.11902/1005.4537.2018.168 OR https://www.jcscp.org/EN/Y2019/V39/I6/536

Fig.1 Schematic diagram of the experimental device for electrochemical hydrogen permeation testing

Fig.2 Procedure of hydrogen microprint

Fig.3 Microstructures of X100 pipeline steel before and after heat treatments: (a) original, (b) furnace cooling, (c) wind cooling

Fig.4 Surface morphologies of X100 pipeline steel after HIC sensitivity test: (a) original, (b) furnace cooling, (c) wind cooling

Table 1 HIC susceptibility parameters of X100 pipeline steel

Fig.5 SEM images of the propagation path of HIC cracks in X100 pipeline steel: (a) original, (b) furnace cooling, (c) wind cooling

Fig.6 BSD images (a~c) and EDS results (d~f) of MnS (a, d), Ca-Al-Si-O (b, e) and MnO (c, f) inclusions associated with HIC cracks in X100 pipeline steel

Fig.7 BSD image (a) and EDS results of points 1 (b) and 2 (c) in Fig.7a around Ca-Al-Si-O inclusion after hydrogen microprint

Fig.8 Electrochemical hydrogen permeation curves of X100 pipeline steel samples: (a) original, (b) furnace cooling, (c) wind cooling

Table 2 Kinetic parameters of hydrogen permeation of X100 pipeline steel samples

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