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Journal of Chinese Society for Corrosion and protection  2017, Vol. 37 Issue (1): 58-62    DOI: 10.11902/1005.4537.2016.193
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Influence of Heat Treatment on Microstructure of Composite Coatings of FeAl-Cr3C2
Yao CHEN1,Honghua ZHANG1,2,Ganlan YANG1,2,Junhuai XIANG1,2()
1 School of Materials and Mechanical & Electrical Engineering, Jiangxi Science and Technology Normal University, Nanchang 330013, China;
2 Jiangxi Key Laboratory of Surface Engineering, Jiangxi Science and Technology Normal University, Nanchang 330013, China
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Abstract  

Composite coatings of Fe40Al-50%Cr3C2 with the thickness of 30 μm were prepared by high velocity oxygen-fuel (HVOF) technology on 304 steel. The change of its microstructure by heat treatment at different temperatures was studied by means of XRD and SEM/EDS. The surface of the coating is very rough and the element distribution is inhomogeneous before the heat treatment. The composition of the coating is mainly composed of Fe, Al, intermetallics plus a little oxide of Fe and Al. A large amount of particles of Fe with big size are present in the outer layer, while a few particles of Al are present in the inner layer. The homogeneity of the coating has great change after vacuum annealing, though some holes still exist in the coating. With the increase of the annealing temperature from 700 ℃ to 900 ℃, the pure Fe and Al particles of big size disappear gradually due to their full diffusion and thereby formation of more intermetallics.

Key words:  thermal spraying      anneal      intermetallic     
Received:  01 October 2016     
Fund: Supported by Natural Science Foundation of Jiangxi Province (20132BAB206015 and 20122BAB216018) and Science and Technology Research Youth Fund Project of Jiangxi Provincial Education Department (GJJ150811)

Cite this article: 

Yao CHEN,Honghua ZHANG,Ganlan YANG,Junhuai XIANG. Influence of Heat Treatment on Microstructure of Composite Coatings of FeAl-Cr3C2. Journal of Chinese Society for Corrosion and protection, 2017, 37(1): 58-62.

URL: 

https://www.jcscp.org/EN/10.11902/1005.4537.2016.193     OR     https://www.jcscp.org/EN/Y2017/V37/I1/58

Fig.1  XRD spectra of the powders and the coatings
Fig.2  XRD patterns of Fe40Al-50%Cr3C2 coatings before and after heat treatment at different temperature
Fig.3  Surface morphology (a) and corresponding element distribution maps of Al (b), O (c), C (d), Fe (e) and Cr (f) of Fe40Al-50%Cr3C2 coatings
Fig.4  SEM surface morphologies (a~d) and section morphologies (e~h) of original coating (a, e) and Fe40Al-50%Cr3C2 coatings after annealed at 700 ℃ (b, f), 800 ℃ (c, g) and 900 ℃ (d, h)
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